By M. R. F. Ashworth
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Additional resources for Analytical Methods for Organic Cyano Groups
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In the test, the sample is treated with a saturated solution of the reagent (sodium salt) and the solution is m a d e faintly alkaline with alkali hydroxide. 13). 37 38 o o Saarivirta and Virtanen< have adapted the reaction to quantitative determination of phenylacetonitrile. An aqueous extract of the sample was allowed to react with the reagent for 4 min at 97-98°. Sodium hydroxide was then added, the mixture left for 20 min at r o o m temperature, and the brown-red colour evaluated colorimetrically with a green filter.
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